PIHKALAnthologyShulgin_page_926

PIHKALAnthologyShulgin | page 926 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

separately from 14 mL isopropylamine in 50 mL hexane treated with 60 mL butyllithium solution. There was an immediate darkening of color. After 15 min stirring, the bromo starting material was gone, by TLC analysis. The reaction mixture was then poured into | L dilute H2SO4. The organic phase was…