PIHKALAnthologyShulgin_page_925

PIHKALAnthologyShulgin | page 925 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

179 4-T-TRIS; 4-THIOTRESCALINE; 4- THIOTRISESCALINE; 3,5-DIETHOXY-4- ETHYLTHIOPHENETHYLAMINE SYNTHESIS: A solution of 12.1 g N,N,NU,NU-tetramethylethylenediamine and 16.6 g of 1,3- diethoxybenzene was made in 200 mL 30-60 !C petroleum ether. This was stirred vigorously under a He atmosphere and…