PIHKALAnthologyShulgin_page_923

PIHKALAnthologyShulgin | page 923 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

was required). The reaction mixture was added to 500 mL H2O containing 4 g sodium hydrosulfite. This was extracted with 3x75 mL petroleum ether, and the pooled extracts stripped of solvent under vacuum to yield 24.5 g of crude 1-(3,4-diethoxy-5-ethylthiophenyl)-2-iodoethane as a viscous yellow oil.…