PIHKALAnthologyShulgin_page_922

PIHKALAnthologyShulgin | page 922 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

178 3-T-TRIS; 3-THIOTRESCALINE; 3- THIOTRISESCALINE; 3,4-DIETHOXY-5- ETHYLTHIOPHENETHYLAMINE SYNTHESIS: A solution of 11.5 g 3-bromo-N-cyclohexyl-4,5-diethoxybenzylidenimine (see under ASB for its preparation) in 150 mL anhydrous Et2O was placed in a He atmosphere, well stirred, and cooled in an…