PIHKALAnthologyShulgin_page_920

PIHKALAnthologyShulgin | page 920 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

177 4-TSB; 4-THIOSYMBESCALINE; 3,5-DIETHOXY-4-METHYLTHIOPHENETHYLAMINE SYNTHESIS: A solution of 12.1 g N,N,NU,NU-tetramethylethylenediamine and 16.6 g of 1,3- diethoxybenzene was made in 200 mL 30-60 !C petroleum ether. This was stirred vigorously under a N2 atmosphere and cooled to 0 !C with an…