PIHKALAnthologyShulgin_page_917

PIHKALAnthologyShulgin | page 917 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

176 3-TSB; 3-THIOSYMBESCALINE; 3-ETHOXY-5-ETHYLTHIO-4-METHOX YPHENETHYLAMINE SYNTHESIS: A solution of 13.4 g 3-bromo-N-cyclohexyl-4-methoxy-5-ethoxybenzylidenimine (see under ME for its preparation) in 150 mL anhydrous Et2O was placed ina He atmosphere, well stirred, and cooled in an external dry…