PIHKALAnthologyShulgin_page_916

PIHKALAnthologyShulgin | page 916 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

400 mL dilute H2SO4. This was washed with 2x75 mL CH2C12, the aqueous phase made basic with aqueous. NaOH, and the product extracted with 2x75 mL CH2C12. These extracts were pooled, the solvent removed under vacuum, and the residue distilled at 115-135 !C at 0.4 mm/Hg to give a white oil. This was…