PIHKALAnthologyShulgin_page_915

PIHKALAnthologyShulgin | page 915 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

175 TRIS; TRESCALINE; TRISESCALINE; 3,4,5-TRIETHOX YPHENETHYLAMINE SYNTHESIS: A solution of 16.9 g of ethyl 3,4,5-triethoxybenzoate in 25 mL THF was added to a well stirred suspension of 8 g LAH in 150 mL THF. The mixture was heated at reflux for 24 h and and, after cooling, treated with IPA to…