PIHKALAnthologyShulgin_page_913

PIHKALAnthologyShulgin | page 913 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

and weighed 0.7 g and was discarded. The second fraction came over at 148-178 !C and weighed 3.0 g. By thin layer chromatography this fraction was about 80% pure, and was used as such in the following reduction. A small sample was ground under methyl cyclopentane yielding white crystals of…