PIHKALAnthologyShulgin_page_904

PIHKALAnthologyShulgin | page 904 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

Recrystallization from 10 mL boiling MeOH gave 0.7 g of 1-(5-methoxy-4-methyl-2-methylthiophenyl)-2- nitropropene with a mp of 83-84 !C. Anal. (C12H15NO3S) C,H. The alternate method for the formation of nitrostyrenes, the reaction of the benzaldehyde in nitroethane as both reagent and solvent, with…