PIHKALAnthologyShulgin_page_903

PIHKALAnthologyShulgin | page 903 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

melted at 135-136 !C. To a slurry of 300 mL cracked ice and 75 mL concentrated H2SO4 in a round- bottomed flask equipped with a reflux condenser, there was added 43 g of the slightly wet 4-methoxy-3- methylbenzenesulfonyl chloride followed by 75 g elemental zinc dust. The temperature was raised to…