PIHKALAnthologyShulgin_page_898

PIHKALAnthologyShulgin | page 898 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

170 5-TOET; 4-ETHYL-2-METHOXY-5- METHYLTHIOAMPHETAMINE SYNTHESIS: A solution of 25 g 3-ethylphenol in 100 mL Et2O was equipped with a magnetic stirrer, and cooled to 0 !C with an external ice bath. There was added 16 mL DMSO. Then, a total of 15 mL chlorosulfonic acid was added dropwise, over the…