PIHKALAnthologyShulgin_page_896

PIHKALAnthologyShulgin | page 896 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

To a solution of 1.5 g LAH in 30 mL anhydrous THF that was cooled to 0 !C and stirred under a He atmosphere, there was added, slowly, 1.05 mL freshly prepared 100% H2S04 (prepared by adding 0.9 g 20% fuming H2SO4 to 1.0 g 96% concentrated H2SO4). This was followed by the addition of a solution of…