PIHKALAnthologyShulgin_page_890

PIHKALAnthologyShulgin | page 890 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

H20 washed and, after sucking as dry as possible, recrystallized from 30 mL boiling MeOH. This provided 1.9 g of 6-formyl-5-methoxy- 1,3-benzoxathiol as brownish needles that melted at 119-120 !C. A solution of 1.5 g 6-formyl-5-methoxy- 1,3-benzoxathiol in 50 mL nitroethane was treated with 0.3 g…