PIHKALAnthologyShulgin_page_886

PIHKALAnthologyShulgin | page 886 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

166 2T-MMDA-3a; 3,4-METHYLENEDIOXY- 2-METHYLTHIOAMPHETAMINE SYNTHESIS: A solution of 30 g piperonal in 25 mL cyclohexylamine was brought to a boil ona hot plate, until there was no more water apparently being evolved. The resulting melt was distilled giving 45 g of…