PIHKALAnthologyShulgin_page_885

PIHKALAnthologyShulgin | page 885 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

the steam bath, then cooled again and stirred for an additional | h. IPA was carefully added to decompose the excess hydride followed by sufficient 10% NaOH to convert the aluminum oxide to a white, easily filterable mass. This was filtered, the filter cake washed with additional IPA, and the…