PIHKALAnthologyShulgin_page_884

PIHKALAnthologyShulgin | page 884 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

165 5-TME; 5-THIOMETAESCALINE; 3-ETHOXY-4-METHOXY-5-METHYLTHIOPHENETHYLAMINE SYNTHESIS: A solution of 10.4 g of 3-bromo-N-cyclohexyl-4-methoxy-5-ethoxybenzylidenimine (see under ME for its preparation) in 150 mL anhydrous Et2O ina He atmosphere was cooled with an external dry ice acetone bath to…