PIHKALAnthologyShulgin_page_883

PIHKALAnthologyShulgin | page 883 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

with dry ice. This fraction was recrystallized from 10 mL MeOH, filtered, and washed sparingly with cold MeOH. After air drying, there was obtained 0.5 g 3-ethoxy-5-methoxy-4- methylthiophenylacetonitrile which had a mp of 65-66 !C. Anal. (C12H1I5NO2S) C,H. A suspension of 0.5 g LAH in 50 mL…