PIHKALAnthologyShulgin_page_882

PIHKALAnthologyShulgin | page 882 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

164 4-TME; 4-THIOMETAESCALINE; 3-ETHOXY-5-METHOXY-4-METHYLTHIOPHENETHYLAMINE SYNTHESIS: A solution of 5.1 g N,N,NU,NU-tetramethylethylenediamine and 6.8 g of 3-ethoxyanisole was dissolved in 80 mL hexane. This was stirred vigorously under a He atmosphere and cooled to 0 !C with an external ice…