PIHKALAnthologyShulgin_page_880

PIHKALAnthologyShulgin | page 880 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

solvent removed under vacuum to yield a residue of a colorless oil. This was distilled at 160-170 !C at 1.0 mn/Hg yielding 2.6 g ofa colorless liquid. This was dissolved in 12 mL IPA, neutralized with 24 drops of concentrated HCI and diluted with 25 mL anhydrous Et2O. The clear solution was…