PIHKALAnthologyShulgin_page_879

PIHKALAnthologyShulgin | page 879 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

163 3-TME; 3-THIOMETAESCALINE; 4,5-DIMETHOXY-3-ETHYLTHIOPHENETHYLAMINE) SYNTHESIS: A solution of 13.0 g of 3-bromo-N-cyclohexyl-4,5-dimethoxybenzylidenimine (see under MP for its preparation) in 125 mL anhydrous Et2O ina He atmosphere was cooled with an external dry ice acetone bath to -80 !C with…