PIHKALAnthologyShulgin_page_875

PIHKALAnthologyShulgin | page 875 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

162 TMA-6; 2,4,6- TRIMETHOXYAMPHETAMINE SYNTHESIS: To a solution of 100 g phloroglucinol dihydrate in 320 mL MeOH there was added 55 mL of concentrated H2SO4, and the clear solution held under reflux conditions overnight. After cooling, there was added 500 mL H20, and the bulk of the MeOH was…