PIHKALAnthologyShulgin_page_873

PIHKALAnthologyShulgin | page 873 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

There was then added 6.5 g tetranitromethane over the course of | min, the stirring was continued for an additional 2 min, and then the reaction mixture was quenched by the addition of 2.2 g KOH in 40 mL H20. There was additional H2O added, and the organics were extracted with 3x75 mL CH2C12. The…