PIHKALAnthologyShulgin_page_872

PIHKALAnthologyShulgin | page 872 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

161 TMA-5; 2,3,6- TRIMETHOXYAMPHETAMINE SYNTHESIS: A solution of 100 g 1,2,4-trimethoxybenzene in 1 L hexane was cooled to 15 !C and treated with 400 mL ofa 15% solution of n-butyllithium in hexane. A white precipitate formed immediately, and stirring was continued for an additional 2 h while the…