PIHKALAnthologyShulgin_page_868

PIHKALAnthologyShulgin | page 868 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

160 TMA-4; 2,3,5- TRIMETHOXYAMPHETAMINE SYNTHESIS: To a solution of 68 g 2,4-dimethoxybenzaldehyde in 250 mL glacial acetic acid that had been warmed to 25 !C and well stirred, there was added, dropwise, 86 g ofa 40% peracetic acid solution (in acetic acid). The reaction was exothermic, and the…