PIHKALAnthologyShulgin_page_862

PIHKALAnthologyShulgin | page 862 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

158 TMA-2; 2,4,5- TRIMETHOXYAMPHETAMINE SYNTHESIS: To a solution of 50 g 2,4,5-trimethoxybenzaldehyde in 175 mL nitroethane there was added 10 g anhydrous ammonium acetate and the mixture was heated on the steam bath for 2 h. The excess nitroethane was removed under vacuum, and the deep orange oily…