PIHKALAnthologyShulgin_page_856

PIHKALAnthologyShulgin | page 856 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

NaOH, and the aqueous washes were pooled with the original base phase. The organic phase was stripped of its CH2C12 under vacuum to give an oil that was dissolved in 40 mL IPA, neutralized with concentrated HCI, and diluted with 400 mL anhydrous Et2O. There was the immediate formation of…