PIHKALAnthologyShulgin_page_855

PIHKALAnthologyShulgin | page 855 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

157 TMA: 3,4,5- TRIMETHOXYAMPHETAMINE SYNTHESIS: To a solution of 39.2 g 3,4,5-trimethoxybenzaldehyde in 30 mL warm EtOH there was added 15.7 g nitroethane followed by 1.5 mL n-butylamine. The reaction mixture was allowed to stand at 40 !C for 7 days. With cooling and scratching, fine yellow…