PIHKALAnthologyShulgin_page_851

PIHKALAnthologyShulgin | page 851 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

!C, weighed 1.8 g and spontaneously crystallized. It was triturated under cold MeOH and filtered yielding, after air drying, 1.1 g 3,5-dimethoxy-4- methylthiophenylacetonitrile, which had a mp of 95-96.5 !C, Anal. (C11H13NO2S) C,H. A suspension of 1.0 g LAH in 40 mL anhydrous THF under N2 was…