PIHKALAnthologyShulgin_page_850

PIHKALAnthologyShulgin | page 850 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

156 TM; 4-TM; 4-THIOMESCALINE; 3,5-DIMETHOXY-4-METHYLTHIOPHENETHYLAMINE SYNTHESIS: A solution of 24.2 g N,N,NU,NU-tetramethylethylenediamine and 27.6 g of 1,3- dimethoxybenzene was dissolved in 400 mL anhydrous hexane. This was stirred vigorously under a N2 atmosphere and cooled to 0 !C with an…