PIHKALAnthologyShulgin_page_848

PIHKALAnthologyShulgin | page 848 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

there was added, dropwise, 0.7 mL of 100% H2S04, followed by a solution of 0.7 g 3,4-dimethoxy-5-methylthio-'-nitrostyrene in 10 mL anhydrous THF. The mixture was brought briefly to a reflux, cooled again, and the excess hydride destroyed with H20 in THF, followed by the dropwise addition of 15%…