PIHKALAnthologyShulgin_page_847

PIHKALAnthologyShulgin | page 847 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

155 3-TM; 3-THIOMESCALINE; 3,4- DIMETHOXY-5- METHYLTHIOPHENETHYLAMINE SYNTHESIS: To an ice cold and well stirred solution of 15 g vanillin and 20 g sodium thiocyanate in 150 mL acetic acid there was added, dropwise over the course of 15 min, a solution of 16 g elemental bromine in 40 mL acetic…