PIHKALAnthologyShulgin_page_844

PIHKALAnthologyShulgin | page 844 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

were filtered, washed with Et2O, and air dried. The weight of 2,4-dimethoxy-3-methylthiophenethylamine hydrochloride (3-TIM) was 0.2 g and the mp was 204-206 !C with decomposition. This hydrochloride appeared to be a hemihydrate. Anal. (C11H18CINO2Sa1/2 H20) C,H,N. DOSAGE: greater than 240 mg.…