PIHKALAnthologyShulgin_page_843

PIHKALAnthologyShulgin | page 843 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

153 3-TIM; 3-THIOMESCALINE; 2,4- DIMETHOXY-3- METHYLTHIOPHENETHYLAMINE SYNTHESIS: A mixture of 3.1 g POCI3 2.8 g N-methylformanilide was heated on a steam bath until it was a deep claret color (about 5 min). To this there was then added 3.0 g of 2,6-dimethoxythioanisole (see under 4-TM for its…