PIHKALAnthologyShulgin_page_838

PIHKALAnthologyShulgin | page 838 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

combined, and extracted with 2x100 mL CH2C12. These extracts were pooled with the original organic phase, and the solvents removed under vacuum. The residue was distilled into two fractions at 0.3 mm/Hg. The first fraction boiled at 95-115 !C and weighed 4.9 g. It was made up of several components,…