PIHKALAnthologyShulgin_page_837

PIHKALAnthologyShulgin | page 837 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

151 TE; 4-TE; 4-THIOESCALINE; 3,5- DIMETHOXY-4- ETHYLTHIOPHENETHYLAMINE SYNTHESIS: A solution was made of 45.2 g N,N,NU,NU-tetramethylethylenediamine and 41.4 g of 1,3- dimethoxybenzene in 300 mL hexane. This was stirred vigorously under a He atmosphere and cooled to 0 !C with an external ice bath.…