PIHKALAnthologyShulgin_page_834

PIHKALAnthologyShulgin | page 834 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

150 3-TE; 3-THIOESCALINE; 4-ETHOXY-5-METHOXY-3-METHYLTHIOPHENETHYLAMINE SYNTHESIS: A solution of 10.4 g of 3-bromo-N-cyclohexyl-4-ethoxy-5-methoxybenzylidenimine (see under 3-TASB for its preparation) in 125 mL anhydrous Et2O, in a He atmosphere, was cooled with an external dry ice acetone bath to…