PIHKALAnthologyShulgin_page_831

PIHKALAnthologyShulgin | page 831 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

4-(n)-butylthio-3,5-dimethoxyphenylacetonitrile, was reduced as such without further purification or analysis. A solution of LAH under N2 (20 mL ofa | M solution in anhydrous THF) was cooled to 0 !C and vigorously stirred. There was added, dropwise, 0.53 mL 100% H2S04, followed by 2.0 g 4-(n)-…