PIHKALAnthologyShulgin_page_830

PIHKALAnthologyShulgin | page 830 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

149 TB; 4-THIOBUSCALINE; 3,5- DIMETHOXY-4-(n)- BUTYLTHIOPHENETHYLAMINE SYNTHESIS: A solution was made of 12.1 g N,N,NU,NU-tetramethylethylenediamine and 13.8 g of 1,3- dimethoxybenzene in 200 mL 30-60 !C petroleum ether. This was stirred vigorously under a He atmosphere and cooled to 0 !C with an…