PIHKALAnthologyShulgin_page_828

PIHKALAnthologyShulgin | page 828 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

to discharge the residual iodine color (about 4 mL was required). The reaction mixture was added to 500 mL water, and sodium hydrosulfite was added to discharge the remaining iodine color (about 4 g). This was extracted with 3x100 mL petroleum ether, the extracts pooled, and the solvent removed…