PIHKALAnthologyShulgin_page_827

PIHKALAnthologyShulgin | page 827 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

148 5-TASB; 5-THIOASYMBESCALINE; 3,4-DIETHOXY-5-METHYLTHIOPHENETHYLAMINE SYNTHESIS: A solution of 11.5 g 3-bromo-N-cyclohexyl-4,5-diethoxybenzylidinimine (see under ASB for its preparation) in 150 mL anhydrous Et2O was placed ina He atmosphere, well stirred, and cooled in an external dry…