PIHKALAnthologyShulgin_page_824

PIHKALAnthologyShulgin | page 824 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

147 4-TASB; 4-THIOASYMBESCALINE; 3-ETHOXY-4-ETHYLTHIO-5-METHOXY PHENETHYLAMINE SYNTHESIS: A solution of 20.5 g N,N,NU,NU-tetramethylethylenediamine and 22.3 g of 3-ethoxyanisole was made in 100 mL hexane under a He atmosphere with good stirring. There was added 125 mL 1.6 M butyllithium in hexane,…