PIHKALAnthologyShulgin_page_821

PIHKALAnthologyShulgin | page 821 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

CH2C12, the extracts pooled, washed first with dilute HCl, then with saturated brine, and the solvent removed under vacuum. The residue was an amber oil weighing 20.4 g, and was distilled at 130-140 !C at 0.3 mm/Hg to yield 12.9 g of 4-ethoxy-3-ethylthio-5-methoxybenzaldehyde as a straw colored oil…