PIHKALAnthologyShulgin_page_820

PIHKALAnthologyShulgin | page 820 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

146 3-TASB; 3-THIOASYMBESCALINE; 4-ETHOXY-3-ETHYLTHIO-5-METHOXYPHENETHYLAMINE SYNTHESIS: Without any solvent, there was combined 21.7 g of solid 5-bromovanillin and 11.4 mL cyclohexylamine. There was the immediate generation of a yellow color and the evolution of heat. The largely solid mass was…