PIHKALAnthologyShulgin_page_815

PIHKALAnthologyShulgin | page 815 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

3,5-diethoxy-4-methoxyphenylacetonitrile as a solid. This weighed 1.3 g and had a mp of 58-59 !C. Anal. (C13H17NO3) C,H. To 30 mL ofa | M solution LAH in THF that had been cooled to 0 !C with vigorous stirring, under a He atmosphere, there was added dropwise 0.78 mL of 100% H2S04. When the addition…