PIHKALAnthologyShulgin_page_814

PIHKALAnthologyShulgin | page 814 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

144 SB; SYMBESCALINE; 3,5-DIETHOXY-4- METHOXY PHENETHYLAMINE SYNTHESIS: A solution of 15 g 1,3-diethoxybenzene and 15 mL of N,N,NU,NU- tetramethylethylenediamine in 200 mL anhydrous Et2O was placed in a He atmosphere, magnetically stirred, and cooled to 0 !C with an ice bath. Over the course of 10…