PIHKALAnthologyShulgin_page_788

PIHKALAnthologyShulgin | page 788 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

from EtOH raised this mp to 109.5-110.5 IC, A suspension of 2.2 g LAH in 300 mL anhydrous Et2O under an inert atmosphere was brought to a gentle reflux. The reflux condensate was passed through a modified Soxhlet thimble containing 1.95 g 1-(2- methoxy-3,4-methylenedioxyphenyl)-2-nitropropene…