PIHKALAnthologyShulgin_page_787

PIHKALAnthologyShulgin | page 787 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

134 MMDA-3a; 2-METHOXY-3,4- METHYLENEDIOXYAMPHETAMINE SYNTHESIS: To a solution of 100 g of 2,3-dihydroxyanisole in 1 L dry acetone there was added 110 g of powdered anhydrous K2CO3 followed by 210 g of methylene iodide. This was brought up to a reflux on the steam bath. There was a sudden…