PIHKALAnthologyShulgin_page_785

PIHKALAnthologyShulgin | page 785 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

The addition required 2 h and the reflux was maintained for 36 h. The reaction mixture was then cooled in an ice bath and there was added, in sequence and commensurate with heat evolution, 36 mL H20, 36 mL 15% NaOH, and finally 108 mL H2O. The granular solids were removed by filtration and washed…