PIHKALAnthologyShulgin_page_784

PIHKALAnthologyShulgin | page 784 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

133 MMDA-2; 2-METHOXY-4,5- METHYLENEDIOXYAMPHETAMINE SYNTHESIS: A solution of 11.5 g pellet KOH (85%) in 75 mL EtOH was treated with 25 g sesamol followed by 27 g methyl iodide. This was brought to reflux on the steam bath. Salt formation was apparent in 20 min, and refluxing was main-tained for a…